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Nuclear Training Services Ltd.
Modules for On-Line Practical Gamma Spectrometry Course |
Level 1: Basics of Radioactivity
- 1.1 The Structure of Atoms and the Chart of the Nuclides
- Structure of the atom, Definitions, Nuclide notation, Chart of the Nuclides, isotopes and nuclides, isobars.
- 1.2 Why some Nuclei decay and how.
- Mass/energy equivalence, changes in mass driving decay, beta minus decay, beta plus decay, electron capture, isobar parabolas, alpha decay, spontaneous fission, differential half-lives, minor decay modes.
- 1.3 Origins of Gamma-Rays, X-rays and other Electromagnetic Radiations
- Nuclear energy levels, deexcitation after beta-, beta+ and alpha decay, lifetime of nuclear levels, metastable states and isomeric transition, X-rays and Auger cascades, X-rays a consequence of electron capture and internal conversion, Annihilation radiation, Bremsstrahlung
- 1.4 Practical Exercise: Retrieving Nuclear Data On-line
- 1.5 Mathematics of Growth and Decay
- Decay equation, specific activity, decay during counting, growth of decay in reactors, growth from a parent, transient equilibrium, secular equilibrium, no equilibrium situations.
- 1.6 Statistics of Counting
- Measurement and Estimates, Standard deviation and variance, Statistical statements, Counting distributions, Sampling statistics, Confidence Limits, Peak area measurement and its uncertainty.
Level 2: Introduction to Gamma-Ray Spectrometry
- 2.1 Gamma-Spectrometry - Why we do it, the Basic System
- 2.2 Practical Exercise: Installation and Use of the CompAct Virtual Gamma Spectrometer.
- Installation, using the display functions, getting information about the spectrum, loading a virtual sample, setting up a count and measuring the count rate.
- 2.3 Practical Exercise: The Gamma-Ray Spectrum and its Interpretation
- Spectrum measurement, total and full energy peak areas.
- 2.4 Practical Exercise: High and Low Resolution Spectrometry
- Comparing High and Low Resolution spectra
- 2.5 Practical Exercise: Decay and Growth: Measurement of half-life
- Plot the decay of a source and estimate the half-life, ot the growth of a source and again estimate the half-life
- 2.6 Practical Exercise: Uncertainty of Counts and Peak Areas
- Take multiple measurements and calculate mean, standard deviations etc. for single (ROI) counts and for peak areas.
Level 3: Gamma-Ray Detectors and Systems
- 3.1 Interactions of Gamma Radiation with Matter
- Practical Exercise: Identification of features in gamma-ray spectra
- 3.2 Semiconductor Detectors for Gamma Spectrometry
- The nature of semiconductors, principles of operation, detector types available, detector mounting, uses of n-type detectors, electrical cooling
- 3.3 Scintillation Detectors
- The nature of scintillators, principles of operation, detector types available, detector mounting, examples of their use.
- 3.4 Origins and Control of Resolution
Sources of uncertainty in gamma-ray detection and measurement. Application to high resolution and scintillation detector systems.
- 3.5 Pulse Processing
- General Layout of the System, Putting the System together, Preamplifiers, Amplifiers and their functions.
- 3.6 MCA's and ADC's and DSP
- 3.7 Practical (Detective) Exercise: Examination and diagnosis of Faulty Spectra.
Level 4: Calibration and use of Gamma Spectrometers
- 4.1 Practical Exercise: Energy Calibration
- 4.2 Practical Exercise: Peak Width (FWHM) Calibration
- 4.3 Practical Exercise: Efficiency Calibration
- 4.4 Calibration Errors - True Coincidence Summing
- Reasons for summing errors, Cascades in decay schemes, solution to the problem, error free calibrations
- 4.5 Interpretation of and checking the Detector Specification
- Practical Exercise: Checking the manufacturers specification
- 4.6 Practical Exercise: Influence of source shape, density and distance on count rate
Level 5: Advanced topics in Gamma Spectrometry
- 5.1 Optimising the counting scheme
- Optimum background width, spectrum size and counting time
- 5.2 Decision Limits and MDA
- Critical Limit, Upper Limit, Critical Limit, Minimum Detectable Activity, When to use which limit. Practical Exercise: Decision Limit Calculations
- 5.3 Use of computers for Spectrum Analysis
- 5.4 Ensuring Quality in Gamma-Ray Spectrometry
- 5.5 Practical Exercise: identification of radionuclides
- 5.6 Practical Exercise: corrections for random summing
- 5.7 Practical Exercise: corrections for density
- 5.8 Observations on measuring environmental samples: Is bigger really better?
- 5.9 Combining results and propagation of uncertainties
- 5.10 Alternative Detector Materials
Resources
- CompAct Virtual Gamma-ray Spectrometer and Spectrum analysis program
- Graph papers -- wmf and Powerpoint files
- List of peaks expected in background spectra
- Ordered list of element names, symbols and atomic numbers (html)
- List of X-ray energies - html and .xls
- Data page: nuclear constants, statistical factors
- Spreadsheet - decay calculations, number of atoms etc.
- Spreadsheet - atomic masses, including calculation of decay energies
- 'Diagnostic kit' for use with fault identification spectra
© Details, course format and programme copyright Dr Gordon Gilmore, who asserts all intellectual property rights.
http://online.nucleartraining.co.uk/modules.htm Copyright © 2000 Dr Gordon Gilmore
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